But du cours
Students must be able to select and implement experimental techniques for analyzing liquid or solid samples. This module should be taught through problem-based learning (PBL) scenarios.
Acquis d'apprentissage visés
- Be able to perform solvent extraction.
- Be able to perform fractional distillation.
- Be able to perform recrystallization.
- Be able to use a rotary evaporator (Rotavap) and describe its operation.
- Be able to use a Kofler bench.
- Be able to measure an optical index.
- Be able to analyze an NMR spectrum.
Prérequis
Chemical equilibria (TC)Organic Chemistry II
Programme
- Extraction Techniques
- Separating funnel.
- Continuous extraction using a Soxhlet apparatus.
- Purification Techniques
- Fractional distillation.
- Recrystallization.
- Rotary evaporator.
- Identification Techniques
- Melting point.
- Optical index.
- Optical rotation.
- TLC (Thin Layer Chromatography).
- Spectroscopy: analysis of provided IR and NMR spectra.
- Titration Methods
- Calibration-based titration.
- Direct or indirect titration.
Modalités d'évaluation
2 Written exams (2h/2h) + 1 Lab report